Structural suppression of blister formation on the tungsten surface under + implantation with an energy of 30 keV

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Abstract

The influence of ultrafine-grained structure and cone-shaped surface morphology on the formation of blisters under irradiation of tungsten with He+ ions with energy of 30 keV has been studied. In comparative experiments, ultrafine-grained and fine-grained samples with an average grain size of 300 nm and 7 μm, respectively, with smooth and cone-shaped surface morphology were used. The ultrafine-grained structure in tungsten samples was obtained by severe plastic deformation, and the cone-shaped surface morphology was obtained by high-fluence irradiation with Ar+ ions with the energy of 30 keV. It was found that blisters are formed on both fine-grained and ultrafine-grained samples when irradiated with He+ ions with a fluence of 1018 ion/cm2. On the fine-grained samples, some of the blisters were with the lids removed, while in the ultrafine-grained samples, all blisters were intact. The thickness of the lids, diameter of the blisters depends on the grain size. The cone-shaped surface morphology on ultrafine-grained tungsten was found to suppress blister formation.

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About the authors

R. Kh. Khisamov

Institute for Metals Superplasticity Problems RAS

Author for correspondence.
Email: r.khisamov@mail.ru
Russian Federation, Ufa

N. N. Andrianova

Lomonosov Moscow State University, Skobeltsyn Institute of Nuclear Physics; Moscow Aviation Institute

Email: r.khisamov@mail.ru
Russian Federation, Moscow; Moscow

A. M. Borisov

Institute for Metals Superplasticity Problems RAS; Lomonosov Moscow State University, Skobeltsyn Institute of Nuclear Physics; Moscow Aviation Institute

Email: r.khisamov@mail.ru
Russian Federation, Ufa; Moscow; Moscow

M. А. Ovchinnikov

Institute for Metals Superplasticity Problems RAS; Lomonosov Moscow State University, Skobeltsyn Institute of Nuclear Physics

Email: r.khisamov@mail.ru
Russian Federation, Ufa; Moscow

I. I. Musabirov

Institute for Metals Superplasticity Problems RAS

Email: r.khisamov@mail.ru
Russian Federation, Ufa

R. R. Timiryaev

Institute for Metals Superplasticity Problems RAS

Email: r.khisamov@mail.ru
Russian Federation, Ufa

R. R. Mulyukov

Institute for Metals Superplasticity Problems RAS

Email: r.khisamov@mail.ru
Russian Federation, Ufa

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Supplementary files

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2. Fig. 1. SEM images obtained in the backscattered electron detection mode of the morphology of the initial (ingot) (a); ultrafine-grained (b); fine-grained (c) tungsten samples.

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3. Fig. 2. SEM images obtained in the secondary electron detection mode of the surface of fine-grained (a) and ultrafine-grained (b, c) tungsten samples after irradiation with He+ ions.

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4. Fig. 3. SEM images obtained in the secondary electron detection mode of the surface layer of fine-grained (a) and ultrafine-grained (b) tungsten samples irradiated with He+ ions.

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5. Fig. 4. SEM images obtained in the secondary electron detection mode at an angle of 45°: fine-grained (a) and ultrafine-grained (b) tungsten samples after irradiation with Ar+ ions.

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6. Fig. 5. SEM images obtained at an angle of 45°: fine-grained (a, b) and ultrafine-grained (c, d) tungsten samples after preliminary irradiation with Ar+ and subsequent irradiation with He+.

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